Allyl 2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Base Information

Chemical Name:Allyl 2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside
CAS No.:153658-80-1
Molecular Formula:C₂₇H₃₇NO₆Si
Molecular Weight:499.679
Hs Code.:

Synonyms:Allyl 2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

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Chemical Property of Allyl 2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

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Technology Process of Allyl 2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

There total 2 articles about Allyl 2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 54400-75-8,64650-83-5,88903-97-3,116347-86-5,140849-88-3,144300-01-6,54400-77-0
allyl 2-acetamido-2-deoxy-β-D-glucopyranoside

: 58479-61-1
tert-butylchlorodiphenylsilane

: 153658-80-1
Allyl 2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 10h; Ambient temperature;
DOI:10.1021/jo00083a032

Reference yield:

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 153658-80-1
Allyl 2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / allyl alcohol / 0.5 h / 20 °C

2: 88 percent / pyridine / 6 h / 20 °C

With pyridine; allyl alcohol; 1: Substitution / 2: Substitution;
DOI:10.1080/07328309908544034

Reference yield: 72.0%

: 153658-80-1
Allyl 2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

: Dibenzyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl phosphite

: 153658-83-4
Allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1,3)-2-acetamido-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Guidance literature:: With molecular sieve; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1021/jo00083a032