(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester

Base Information

Chemical Name:(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester
CAS No.:218443-23-3
Molecular Formula:C₄₀H₄₀N₂O₁₀
Molecular Weight:708.765
Hs Code.:

Synonyms:(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester

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Chemical Property of (S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester

Chemical Property:

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Technology Process of (S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester

There total 5 articles about (S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 218443-23-3
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / NaHCO₃ / H₂O; dioxane / 8 h / 0 - 20 °C

2: LiOH / H₂O; dioxane / Ambient temperature

3: H₂O; dioxane / 96 h

With lithium hydroxide; sodium hydrogencarbonate; In 1,4-dioxane; water;
DOI:10.1002/(SICI)1522-2675(19981111)81:11<2053::AID-HLCA2053>3.0.CO;2-4

Reference yield:

: 73872-72-7
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester

: 218443-23-3
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiOH / H₂O; dioxane / Ambient temperature

2: H₂O; dioxane / 96 h

With lithium hydroxide; In 1,4-dioxane; water;
DOI:10.1002/(SICI)1522-2675(19981111)81:11<2053::AID-HLCA2053>3.0.CO;2-4

Reference yield:

: 218443-11-9
(S,S)-diaminooctanedioic acid dimethyl ester

: 218443-23-3
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid bis(2-oxo-2-phenylethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / NaHCO₃ / H₂O; dioxane / 8 h / 0 - 20 °C

2: LiOH / H₂O; dioxane / Ambient temperature

3: H₂O; dioxane / 96 h

With lithium hydroxide; sodium hydrogencarbonate; In 1,4-dioxane; water;
DOI:10.1002/(SICI)1522-2675(19981111)81:11<2053::AID-HLCA2053>3.0.CO;2-4