C₂₂H₂₀ClN₅OS

Base Information

Chemical Name:C₂₂H₂₀ClN₅OS
CAS No.:1425044-63-8
Molecular Formula:C₂₂H₂₀ClN₅OS
Molecular Weight:437.953
Hs Code.:

C<sub>22</sub>H<sub>20</sub>ClN<sub>5</sub>OS

Synonyms:C₂₂H₂₀ClN₅OS

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Chemical Property of C₂₂H₂₀ClN₅OS

Chemical Property:

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Technology Process of C₂₂H₂₀ClN₅OS

There total 5 articles about C₂₂H₂₀ClN₅OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1425044-60-5
(S)-3-(1-((2-amino-5-iodopyrimidin-4-yl)amino)ethyl)-8-chloro-2-phenylisoquinolin-1(2H)-one

: 5188-07-8
sodium thiomethoxide

: 1425044-63-8
C₂₂H₂₀ClN₅OS

Guidance literature:: With copper(l) iodide; sodium carbonate; In isopropyl alcohol; at 80 ℃; for 24h; Sealed tube;

Reference yield:

: 1386861-46-6
2-chloro-6-methyl-N-phenylbenzamide

: 1425044-63-8
C₂₂H₂₀ClN₅OS

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere

1.2: 2 h / -30 - -10 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 16 h / 120 °C / Sealed tube

3.1: sodium carbonate; copper(l) iodide / isopropyl alcohol / 24 h / 80 °C / Sealed tube

With copper(l) iodide; n-butyllithium; sodium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; hexane; isopropyl alcohol;

Reference yield:

: 62-53-3
aniline

: 1425044-63-8
C₂₂H₂₀ClN₅OS

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

1.2: 2 h / 20 - 40 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere

2.2: 2 h / -30 - -10 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 16 h / 120 °C / Sealed tube

4.1: sodium carbonate; copper(l) iodide / isopropyl alcohol / 24 h / 80 °C / Sealed tube

With copper(l) iodide; n-butyllithium; oxalyl dichloride; sodium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; hexane; dichloromethane; isopropyl alcohol;