Methyl 10-(4-cyclohexylbenzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-8-carboxylate hydrochloride salt

Base Information

• Chemical Name: Methyl 10-(4-cyclohexylbenzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-8-carboxylate hydrochloride salt
• CAS No.: 473911-24-9
• Molecular Formula: C₃₃H₃₈N₄O₄*ClH
• Molecular Weight: 591.15

Synonyms:Methyl 10-(4-cyclohexylbenzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-8-carboxylate hydrochloride salt

Chemical Property of Methyl 10-(4-cyclohexylbenzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-8-carboxylate hydrochloride salt

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Technology Process of Methyl 10-(4-cyclohexylbenzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-8-carboxylate hydrochloride salt

There total 1 articles about Methyl 10-(4-cyclohexylbenzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-8-carboxylate hydrochloride salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-piperazine (109-01-3) + methyl 10-(4-cyclohexylbenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine-8-carboxylate (473911-88-5) + trichloromethyl chloroformate (503-38-8) → Methyl 10-(4-cyclohexylbenzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-8-carboxylate hydrochloride salt (473911-24-9)

Guidance literature:

With hydrogenchloride; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; ethyl acetate;

Reference yield:

methyl 10-(4-cyclohexylbenzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine-8-carboxylate (473911-89-6) + Methyl 10-(4-cyclohexylbenzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-8-carboxylate hydrochloride salt (473911-24-9) → 10-(4-Cyclohexyl-benzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine-8-carboxylic acid (473911-26-1)

Guidance literature:

With hydrogenchloride; sodium hydroxide; In ethanol; dichloromethane;

upstream raw materials:

1-methyl-piperazine

methyl 10-(4-cyclohexylbenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine-8-carboxylate

trichloromethyl chloroformate

Downstream raw materials:

10-(4-Cyclohexyl-benzoyl)-3-[(4-methyl-1-piperazinyl)carbonyl]-10,11-dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepine-8-carboxylic acid

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