Phosphorous acid 2,6-diethyl-phenyl ester 2-ethyl-phenyl ester phenyl ester

Base Information

Chemical Name:Phosphorous acid 2,6-diethyl-phenyl ester 2-ethyl-phenyl ester phenyl ester
CAS No.:100814-84-4
Molecular Formula:C₂₄H₂₇O₃P
Molecular Weight:394.45
Hs Code.:

Synonyms:Phosphorous acid 2,6-diethyl-phenyl ester 2-ethyl-phenyl ester phenyl ester

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Chemical Property of Phosphorous acid 2,6-diethyl-phenyl ester 2-ethyl-phenyl ester phenyl ester

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Technology Process of Phosphorous acid 2,6-diethyl-phenyl ester 2-ethyl-phenyl ester phenyl ester

There total 6 articles about Phosphorous acid 2,6-diethyl-phenyl ester 2-ethyl-phenyl ester phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-95-2,27073-41-2
phenol

: 101-02-0
triphenyl phosphite

: 100814-87-7
Phosphorous acid 2-ethyl-phenyl ester diphenyl ester

: 100814-86-6
Phosphorous acid 2,6-diethyl-phenyl ester diphenyl ester

: 100814-84-4
Phosphorous acid 2,6-diethyl-phenyl ester 2-ethyl-phenyl ester phenyl ester

Guidance literature:: With o-Hydroxyethylbenzene; 2,6-diethylphenol; triethylamine; phosphorus trichloride; In toluene; for 1h; Further byproducts given; Heating;
DOI:10.1021/ja00270a036

Reference yield:

: 108-95-2,27073-41-2
phenol

: 100814-84-4
Phosphorous acid 2,6-diethyl-phenyl ester 2-ethyl-phenyl ester phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 15 percent Chromat_. / <(PhO)3P>4Ru complex, KOPh / tetrahydrofuran / 3.5 h / 177 °C / 4912.9 Torr

2: 21.3 percent Chromat_. / PCl₃, NEt₃, phenol / toluene / 1 h / Heating

With <(PhO)3P>4Ru; potassium phenolate; triethylamine; phosphorus trichloride; phenol; In tetrahydrofuran; toluene;
DOI:10.1021/ja00270a036

Reference yield:

: 90-00-6
o-Hydroxyethylbenzene

: 1006-59-3
2,6-diethylphenol

: 100814-87-7
Phosphorous acid 2-ethyl-phenyl ester diphenyl ester

: 100814-86-6
Phosphorous acid 2,6-diethyl-phenyl ester diphenyl ester

: 100814-84-4
Phosphorous acid 2,6-diethyl-phenyl ester 2-ethyl-phenyl ester phenyl ester

: 100814-83-3
Phosphorous acid bis-(2,6-diethyl-phenyl) ester 2-ethyl-phenyl ester

Guidance literature:: With triethylamine; phosphorus trichloride; phenol; In toluene; for 1h; Further byproducts given; Heating;
DOI:10.1021/ja00270a036