3,4,5,6-Tetrafluoro-phthalic acid mono-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl) ester

Base Information

Chemical Name:3,4,5,6-Tetrafluoro-phthalic acid mono-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl) ester
CAS No.:851963-38-7
Molecular Formula:C₃₆H₃₂F₄O₉
Molecular Weight:684.638
Hs Code.:

Synonyms:3,4,5,6-Tetrafluoro-phthalic acid mono-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl) ester

Suppliers and Price of 3,4,5,6-Tetrafluoro-phthalic acid mono-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,4,5,6-Tetrafluoro-phthalic acid mono-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,4,5,6-Tetrafluoro-phthalic acid mono-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl) ester

There total 1 articles about 3,4,5,6-Tetrafluoro-phthalic acid mono-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 851963-21-8
(2,2,2-Trichloro-acetyl)-carbamic acid (2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl ester

: 851963-38-7
3,4,5,6-Tetrafluoro-phthalic acid mono-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: polystyrene-bound [1,3,2]diazaphosphorinane / CH₂Cl₂ / 0.17 h / 20 °C

1.2: KOH / methanol / 3 h / 60 °C

2.1: 4-(dimethylamino)pyridine; pyridine / 18 h / 20 °C

With pyridine; dmap; polystyrene-bound [1,3,2]diazaphosphorinane; In dichloromethane;
DOI:10.1002/anie.200462422