N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-6-aminohexanoic acid

Base Information

Chemical Name:N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-6-aminohexanoic acid
CAS No.:910488-00-5
Molecular Formula:C₂₉H₂₉NO₅
Molecular Weight:471.553
Hs Code.:

Synonyms:N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-6-aminohexanoic acid

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Chemical Property of N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-6-aminohexanoic acid

Chemical Property:

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Technology Process of N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-6-aminohexanoic acid

There total 6 articles about N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-6-aminohexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910488-32-3
2,3-methyIenedioxy-6-benzyloxy-phenanthrene-9-carboxylic acid

: 910488-00-5
N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-6-aminohexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 4-(dimethylamino)pyridine; 1-hydroxybenzotriazole; 4-methylmorpholine / N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride / dimethylformamide / 0 - 20 °C

2: borane-dimethylsulfide complex / tetrahydrofuran / 20 °C

3: NaOH / methanol / 4 h / Heating

With 4-methyl-morpholine; dmap; sodium hydroxide; dimethylsulfide borane complex; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.06.009

Reference yield:

methyl 6-aminohexanoate hydrochloride: 2780-89-4
methyl 6-aminohexanoate hydrochloride

: 910488-00-5
N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-6-aminohexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 4-(dimethylamino)pyridine; 1-hydroxybenzotriazole; 4-methylmorpholine / N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride / dimethylformamide / 0 - 20 °C

2: borane-dimethylsulfide complex / tetrahydrofuran / 20 °C

3: NaOH / methanol / 4 h / Heating

With 4-methyl-morpholine; dmap; sodium hydroxide; dimethylsulfide borane complex; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.06.009

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 910488-00-5
N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylmethyl)-6-aminohexanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: acetyl chloride / 2 h / Heating

2: 92 percent / 4-(dimethylamino)pyridine; 1-hydroxybenzotriazole; 4-methylmorpholine / N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride / dimethylformamide / 0 - 20 °C

3: borane-dimethylsulfide complex / tetrahydrofuran / 20 °C

4: NaOH / methanol / 4 h / Heating

With 4-methyl-morpholine; dmap; sodium hydroxide; dimethylsulfide borane complex; benzotriazol-1-ol; acetyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.06.009