methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylcarbonyl)-6-aminohexanoate

Base Information

Chemical Name:methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylcarbonyl)-6-aminohexanoate
CAS No.:910487-98-8
Molecular Formula:C₃₀H₂₉NO₆
Molecular Weight:499.563
Hs Code.:

Synonyms:methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylcarbonyl)-6-aminohexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylcarbonyl)-6-aminohexanoate

Chemical Property:

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Technology Process of methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylcarbonyl)-6-aminohexanoate

There total 2 articles about methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylcarbonyl)-6-aminohexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 910488-32-3
2,3-methyIenedioxy-6-benzyloxy-phenanthrene-9-carboxylic acid

methyl 6-aminohexanoate hydrochloride: 2780-89-4
methyl 6-aminohexanoate hydrochloride

: 910487-98-8
methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylcarbonyl)-6-aminohexanoate

Guidance literature:: With 4-methyl-morpholine; dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2006.06.009

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 910487-98-8
methyl N-(2,3-methylenedioxy-6-benzyloxy-phenanthr-9-ylcarbonyl)-6-aminohexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / 2 h / Heating

2: 92 percent / 4-(dimethylamino)pyridine; 1-hydroxybenzotriazole; 4-methylmorpholine / N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride / dimethylformamide / 0 - 20 °C

With 4-methyl-morpholine; dmap; benzotriazol-1-ol; acetyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.06.009