(1S,2R,3S,5S)-benzoic acid 3-hydroxy-2-hydroxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester

Base Information

Chemical Name:(1S,2R,3S,5S)-benzoic acid 3-hydroxy-2-hydroxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester
CAS No.:183498-51-3
Molecular Formula:C₁₉H₂₂N₂O₆
Molecular Weight:374.393
Hs Code.:

Synonyms:(1S,2R,3S,5S)-benzoic acid 3-hydroxy-2-hydroxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester

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Chemical Property of (1S,2R,3S,5S)-benzoic acid 3-hydroxy-2-hydroxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester

Chemical Property:

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Technology Process of (1S,2R,3S,5S)-benzoic acid 3-hydroxy-2-hydroxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester

There total 7 articles about (1S,2R,3S,5S)-benzoic acid 3-hydroxy-2-hydroxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 183498-48-8
(1S,2R,3S,5S)-benzoic acid 3-benzyloxy-2-benzyloxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester

: 183498-51-3
(1S,2R,3S,5S)-benzoic acid 3-hydroxy-2-hydroxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 5h; under 760 Torr; Ambient temperature;
DOI:10.1016/0040-4020(96)00755-7

Reference yield:

: 132151-65-6
(E)-3-methoxy-2-methylacryloyl isocyanate

: 183498-51-3
(1S,2R,3S,5S)-benzoic acid 3-hydroxy-2-hydroxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / CH₂Cl₂ / 0.5 h / -60 - 20 °C

2: 85 percent / 2 N aq. HCl / ethanol / 20 h / Heating

3: 91 percent / pyridine, DMAP / CH₂Cl₂ / 4 h / Heating

4: hydrogen / 10percent Pd/C / methanol / 5 h / 760 Torr / Ambient temperature

With pyridine; hydrogenchloride; dmap; hydrogen; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1016/0040-4020(96)00755-7

Reference yield:

: 183498-38-6
(1S,2S,3R,4S)-4-benzyloxy-3-benzyloxymethyl-2-(tert-butyl-dimethyl-silanyloxymethyl)-cyclopentylamine

: 183498-51-3
(1S,2R,3S,5S)-benzoic acid 3-hydroxy-2-hydroxymethyl-5-(thymin-1-yl)-cyclopentylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / CH₂Cl₂ / 0.5 h / -60 - 20 °C

2: 85 percent / 2 N aq. HCl / ethanol / 20 h / Heating

3: 91 percent / pyridine, DMAP / CH₂Cl₂ / 4 h / Heating

4: hydrogen / 10percent Pd/C / methanol / 5 h / 760 Torr / Ambient temperature

With pyridine; hydrogenchloride; dmap; hydrogen; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1016/0040-4020(96)00755-7