Im-F₉bp

Base Information

Chemical Name:Im-F₉bp
CAS No.:321724-99-6
Molecular Formula:C₁₅H₃F₉N₂
Molecular Weight:382.188
Hs Code.:

Synonyms:Im-F₉bp

Suppliers and Price of Im-F₉bp

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Im-F₉bp

Chemical Property:

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Technology Process of Im-F₉bp

There total 1 articles about Im-F₉bp which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 288-32-4
1H-imidazole

: 434-90-2
decafluorobiphenyl

: 321724-99-6
Im-F₉bp

: 321725-00-2
Im-F₈bp-Im

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 30 ℃; for 12h;
DOI:10.1021/ja0543088

Reference yield: 14.5%

: 321724-99-6
Im-F₉bp

: 944767-61-7
[(4,7-dimethyl-1,10-phenanthroline)Re(CO)3(THF)][BF₄]

: [(4,7-dimethyl-1,10-phenanthroline)Re(CO)3(NC₃H₃NC₆F₄C₆F₅)][BF₄]

Guidance literature:: In tetrahydrofuran; dichloromethane; Re complex dissolved in CH2Cl2-THF; added to ligand; stirred at 30°C for 48-120 h (monitored by mass spectra); removed from heating; rotary evapd.; oil dissolved in min. CH2Cl2; flash chromd. (silica gel, MeOH-CH2Cl2 3:97 to 40-60); rotary evapd. to dryness;
DOI:10.1021/ja0543088