1D-(1,2,5/3,4)-4-O-benzoyl-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol

Base Information

Chemical Name:1D-(1,2,5/3,4)-4-O-benzoyl-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol
CAS No.:135131-65-6
Molecular Formula:C₂₃H₂₈O₇
Molecular Weight:416.471
Hs Code.:

Synonyms:1D-(1,2,5/3,4)-4-O-benzoyl-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol

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Chemical Property of 1D-(1,2,5/3,4)-4-O-benzoyl-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol

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Technology Process of 1D-(1,2,5/3,4)-4-O-benzoyl-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol

There total 10 articles about 1D-(1,2,5/3,4)-4-O-benzoyl-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 142543-94-0
1D-(1,2,5/3,4)-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol

: 98-88-4
benzoyl chloride

: 135131-65-6
1D-(1,2,5/3,4)-4-O-benzoyl-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol

Guidance literature:: With pyridine; at 70 ℃; for 13h;

Reference yield:

: 58769-23-6
1L-3,4,:5,6-di-O-isopropylidene-2-O-methyl-chiro-inositol

: 135131-65-6
1D-(1,2,5/3,4)-4-O-benzoyl-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol

Guidance literature:: Multi-step reaction with 8 steps

1: 1) NaH / 1) DMF, 0 deg C, 40 min, 2) r.t., 30 min

2: 81 percent / pTsOH*H₂O / methanol / 7 h / 0 °C

3: 1) pyridine, 2) pyridine / 1) 0 deg C, 27 h, 2) r.t., 6 h

4: 84 percent / NaOMe / methanol / 3 h / Ambient temperature

5: 91 percent / LiAlH₄ / tetrahydrofuran / 3 h / Ambient temperature

6: 1) NaH / 1) DMF, 0 deg C, 45 min, 2) r.t., 12 h

7: 92 percent / pTsOH / methanol / 4 h / Ambient temperature

8: 87 percent / pyridine / 13 h / 70 °C

With pyridine; lithium aluminium tetrahydride; sodium methylate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;

Reference yield:

: 135131-63-4
1D-(1,2,5/3,4)-3,4-O-isopropylidene-1,2-di-O-methylcyclohexanepentaol

: 135131-65-6
1D-(1,2,5/3,4)-4-O-benzoyl-5-O-(p-methoxybenzyl)-1,2-di-O-methylcyclohexanepentaol

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH / 1) DMF, 0 deg C, 45 min, 2) r.t., 12 h

2: 92 percent / pTsOH / methanol / 4 h / Ambient temperature

3: 87 percent / pyridine / 13 h / 70 °C

With pyridine; sodium hydride; toluene-4-sulfonic acid; In methanol;