Technology Process of C28H31F2N3O5S2Si
There total 5 articles about C28H31F2N3O5S2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
copper(l) iodide; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0);
at 60 ℃;
for 3h;
Inert atmosphere;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C
1.2: 20 h / 20 °C / Inert atmosphere
1.3: 3 h / 50 °C
2.1: pyridine / 48 h / 20 °C
3.1: triethylamine / triphenylphosphine; copper(l) iodide; bis(dibenzylideneacetone)-palladium(0) / 3 h / 60 °C / Inert atmosphere; Sealed tube
With
pyridine; potassium carbonate; triethylamine;
copper(l) iodide; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0);
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 121 h / -10 - 0 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C
2.2: 20 h / 20 °C / Inert atmosphere
2.3: 3 h / 50 °C
3.1: pyridine / 48 h / 20 °C
4.1: triethylamine / triphenylphosphine; copper(l) iodide; bis(dibenzylideneacetone)-palladium(0) / 3 h / 60 °C / Inert atmosphere; Sealed tube
With
pyridine; potassium carbonate; triethylamine; lithium hexamethyldisilazane;
copper(l) iodide; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; N,N-dimethyl-formamide;