3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane

Base Information

Chemical Name:3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane
CAS No.:869711-07-9
Molecular Formula:C₂₁H₂₂ClFN₄O₃
Molecular Weight:432.882
Hs Code.:

Synonyms:3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane

Suppliers and Price of 3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane

There total 4 articles about 3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 869792-62-1
3β-azido-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane

: 869711-07-9
3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Lindlar catalyst / methanol

2: Et₃N / butan-1-ol / 105 °C

3: Heating

With hydrogen; triethylamine; Lindlar's catalyst; In methanol; butan-1-ol;
DOI:10.1016/j.tetlet.2005.08.163

Reference yield:

: 100101-50-6
<1S-(1α,2β,3α,4α,5β)>-2-azido-3,4-(dimethylmethylenedioxy)-5-<(phenylmethoxy)methyl>-1-cyclopentanol

: 869711-07-9
3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane

Guidance literature:: Multi-step reaction with 4 steps

1.1: Tf₂O / pyridine; CH₂Cl₂

1.2: 85 percent / TASF / tetrahydrofuran

2.1: H₂ / Lindlar catalyst / methanol

3.1: Et₃N / butan-1-ol / 105 °C

4.1: Heating

With trifluoromethylsulfonic anhydride; hydrogen; triethylamine; Lindlar's catalyst; In pyridine; methanol; dichloromethane; butan-1-ol;
DOI:10.1016/j.tetlet.2005.08.163

Reference yield:

: 3β-amino-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxy cyclopentane

: 869711-07-9
3β-(6-chloropurin-9-yl)-4β-fluoro-5β-benzyloxymethyl-1α,2α-isopropylidenedioxycyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / butan-1-ol / 105 °C

2: Heating

With triethylamine; In butan-1-ol;
DOI:10.1016/j.tetlet.2005.08.163