{3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester

Base Information

Chemical Name:{3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester
CAS No.:1134000-27-3
Molecular Formula:C₂₇H₃₇N₃O₆
Molecular Weight:499.607
Hs Code.:

Synonyms:{3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester

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Chemical Property of {3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester

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Technology Process of {3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester

There total 1 articles about {3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-36-2
ethyl bromoacetate

: 103493-32-9
{4-[(3-amino-propyl)-benzyloxycarbonyl-amino]-butyl}-carbamic acid benzyl ester

: 1134000-27-3
{3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester

Guidance literature:: With triethylamine; In acetonitrile; for 4h;

Reference yield: 61.0%

: 1134000-27-3
{3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester

: 501-53-1,94274-21-2
benzyl chloroformate

: 1134000-29-5
(benzyloxycarbonyl-{3-[benzyloxycarbonyl-(4-benzyloxy-carbonylaminobutyl)-amino]-propyl}-amino)-acetic acid ethyl ester

Guidance literature:: {3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester; benzyl chloroformate; With sodium hydrogencarbonate; In n-heptane; water; ethyl acetate; acetone; for 2h;

With hydrogenchloride; In water; acetone;

Reference yield:

: 1134000-27-3
{3-[benzyloxycarbonyl-(4-benzyloxycarbonylaminobutyl)-amino]-propylamino}-acetic acid ethyl ester

: 3-(4-aminobutylamino)-propylamino-N-9-{[4-hydroxy-3,5-dimethoxyphenyl]-8-oxo-5,5a,6,8,8a,9-hexahydrofuro[3',4':6,7]naphtho-2,3-[d]-1,3-dioxol-5-yl}-acetamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / ethyl acetate; n-heptane; water; acetone / 2 h

2.1: sodium hydroxide; ethanol / 1 h / Reflux

3.1: triethylamine / acetonitrile

3.2: 1 h / 20 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol / 3 h

With ethanol; hydrogen; sodium hydrogencarbonate; triethylamine; sodium hydroxide; palladium 10% on activated carbon; In methanol; n-heptane; water; ethyl acetate; acetone; acetonitrile;