tert-butyl (3S,4R)-3,4-bis(benzyloxy)-5-hydroxy-2-methylenepentylcarbamate

Base Information

Chemical Name:tert-butyl (3S,4R)-3,4-bis(benzyloxy)-5-hydroxy-2-methylenepentylcarbamate
CAS No.:1369810-69-4
Molecular Formula:C₂₅H₃₃NO₅
Molecular Weight:427.541
Hs Code.:

Synonyms:tert-butyl (3S,4R)-3,4-bis(benzyloxy)-5-hydroxy-2-methylenepentylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (3S,4R)-3,4-bis(benzyloxy)-5-hydroxy-2-methylenepentylcarbamate

Chemical Property:

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Technology Process of tert-butyl (3S,4R)-3,4-bis(benzyloxy)-5-hydroxy-2-methylenepentylcarbamate

There total 2 articles about tert-butyl (3S,4R)-3,4-bis(benzyloxy)-5-hydroxy-2-methylenepentylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₂₀H₂₅NO₃

: 1369810-69-4
tert-butyl (3S,4R)-3,4-bis(benzyloxy)-5-hydroxy-2-methylenepentylcarbamate

Guidance literature:: With sodium hydrogencarbonate; In ethyl acetate; at 0 - 20 ℃; for 4h;
DOI:10.1039/c2ob06851f

Reference yield:

: N-((4S,5R)-4,5-bis(benzyloxy)-3-methylenetetrahydro-2H-pyran-2-yl)-2,2,2-trichloroacetamide

: 1369810-69-4
tert-butyl (3S,4R)-3,4-bis(benzyloxy)-5-hydroxy-2-methylenepentylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 2 h / 0 - 20 °C

2: sodium hydrogencarbonate / ethyl acetate / 4 h / 0 - 20 °C

With sodium tetrahydroborate; sodium hydrogencarbonate; In ethanol; ethyl acetate;
DOI:10.1039/c2ob06851f