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Technology Process of Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*ClO4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2ClO4

Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*ClO4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2ClO4

Base Information
  • Chemical Name:Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*ClO4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2ClO4
  • CAS No.:154827-79-9
  • Molecular Formula:C64H58Au3P4*ClO4
  • Molecular Weight:1641.41
  • Hs Code.:
Au<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=Au<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2ClO<sub>4</sub>

Synonyms:Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*ClO4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2ClO4

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Chemical Property of Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*ClO4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2ClO4
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Technology Process of Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*ClO4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2ClO4

There total 1 articles about Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*ClO4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2ClO4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

gold(I)-bis-triphenylphosphino-perchlorate
14853-97-5

gold(I)-bis-triphenylphosphino-perchlorate

[Au2(μ-(CH2)2PPh2)2]

[Au2(μ-(CH2)2PPh2)2]

Au<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=Au<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2ClO<sub>4</sub>
154827-79-9

Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*ClO4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2ClO4

Guidance literature:
In dichloromethane; to a soln. of Au2(μ-CH2PPh2CH2)2 Au(PPh3)ClO4 is added, mixt. is stirred for 6 h; solvent is evapd., addn. of hexane leads to pptn., elem. anal.;

Reference yield: 65.0%

Au<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=Au<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2ClO<sub>4</sub>
154827-79-9

Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*ClO4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2ClO4

Au<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2<sup>(1+)</sup>*C<sub>12</sub>H<sub>4</sub>N<sub>4</sub><sup>(1-)</sup>=Au<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>2</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2C<sub>12</sub>H<sub>4</sub>N<sub>4</sub>

Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2(1+)*C12H4N4(1-)=Au3(CH2P(C6H5)2CH2)2(P(C6H5)3)2C12H4N4

Guidance literature:
With 7,7',8,8'-tetracyanoquinodimethane lithium; In ethanol; to a soln. of Au-compd. LiTCCNQ is added, mixt. is stirred for 10 h at room temp.; ppt. is filtered off, washed with diethyl ether, lem. anal.;
upstream raw materials:

gold(I)-bis-triphenylphosphino-perchlorate

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