(+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne

Base Information

Chemical Name:(+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne
CAS No.:566151-29-9
Molecular Formula:C₂₂H₃₄OSi₂
Molecular Weight:370.682
Hs Code.:

Synonyms:(+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne

Suppliers and Price of (+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne

Chemical Property:

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Technology Process of (+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne

There total 4 articles about (+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54655-07-1
lithium trimethylsilylacetylenide

: 566151-29-9
(+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaOH / CH₂Cl₂

2.1: n-BuLi / tetrahydrofuran; hexane

2.2: boron trifluoride etherate / tetrahydrofuran; hexane

2.3: tetrahydrofuran; hexane

3.1: imidazole / dimethylformamide

With 1H-imidazole; sodium hydroxide; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo034391m

Reference yield:

: 158070-23-6
1-chloro-5-trimethylsilyl-pent-4-yn-2-ol

: 566151-29-9
(+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaOH / CH₂Cl₂

2.1: n-BuLi / tetrahydrofuran; hexane

2.2: boron trifluoride etherate / tetrahydrofuran; hexane

2.3: tetrahydrofuran; hexane

3.1: imidazole / dimethylformamide

With 1H-imidazole; sodium hydroxide; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo034391m

Reference yield:

: 138084-13-6
trimethyl(3-(oxiran-2-yl)prop-1-yn-1-yl)silane

: 566151-29-9
(+/-)-4-[(tert-butyl)dimethylsiloxy]-1-phenyl-7-(trimethylsilyl)-1,6-heptadiyne

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane

1.2: boron trifluoride etherate / tetrahydrofuran; hexane

1.3: tetrahydrofuran; hexane

2.1: imidazole / dimethylformamide

With 1H-imidazole; n-butyllithium; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/jo034391m