phenyl 4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)thio-β-D-gulcopyranoside

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Chemical Name:phenyl 4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)thio-β-D-gulcopyranoside
CAS No.:1415351-33-5
Molecular Formula:C₂₄H₂₃Cl₄NO₇S
Molecular Weight:611.327
Hs Code.:

Synonyms:phenyl 4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)thio-β-D-gulcopyranoside

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Chemical Property of phenyl 4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)thio-β-D-gulcopyranoside

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Technology Process of phenyl 4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)thio-β-D-gulcopyranoside

There total 1 articles about phenyl 4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)thio-β-D-gulcopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 79-04-9
chloroacetyl chloride

: phenyl N-(2,2,2-trichloroethoxy)carbonyl-2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

: 1415351-33-5
phenyl 4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)thio-β-D-gulcopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1016/j.carres.2012.08.008

Reference yield: 73.0%

: 1246851-95-5
2-(trimethylsilyl)ethyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside

: 1415351-33-5
phenyl 4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)thio-β-D-gulcopyranoside

: 1415351-34-6
2-(trimethylsilyl)ethyl 4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-galactopyranosyl-(1→4)-2,3-di-O-benzoyl-6-O-benzyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluoroacetic acid; In dichloromethane; at -40 ℃; for 1h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2012.08.008