2,4-di-tert-butyl-6-bis(2-(diethylamino)ethyl)aminomethylphenol

Base Information

• Chemical Name: 2,4-di-tert-butyl-6-bis(2-(diethylamino)ethyl)aminomethylphenol
• CAS No.: 912573-08-1
• Molecular Formula: C₂₇H₅₁N₃O
• Molecular Weight: 433.721
• Mol file: 912573-08-1.mol

Synonyms:2,4-di-tert-butyl-6-bis(2-(diethylamino)ethyl)aminomethylphenol

Chemical Property of 2,4-di-tert-butyl-6-bis(2-(diethylamino)ethyl)aminomethylphenol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2,4-di-tert-butyl-6-bis(2-(diethylamino)ethyl)aminomethylphenol

There total 1 articles about 2,4-di-tert-butyl-6-bis(2-(diethylamino)ethyl)aminomethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + N,N,N',N'-tetraethyldiethylenetriamine (123-12-6) + 2,4-di-tert-Butylphenol (96-76-4) → 2,4-di-tert-butyl-6-bis(2-(diethylamino)ethyl)aminomethylphenol (912573-08-1)

Guidance literature:

formaldehyd; N,N,N',N'-tetraethyldiethylenetriamine; at 80 ℃;

2,4-di-tert-Butylphenol; In methanol; Heating;

DOI:10.1039/b600939e

Reference yield: 67.0%

2,4-di-tert-butyl-6-bis(2-(diethylamino)ethyl)aminomethylphenol (912573-08-1) → potassium 4,6-di-tert-butyl-2-bis[2-(diethylamino)ethyl]aminomethylphenoxide

Guidance literature:

With potassium hydride; In toluene; at 20 ℃; for 16h;

DOI:10.1039/b607753f

Reference yield: 32.0%

2,4-di-tert-butyl-6-bis(2-(diethylamino)ethyl)aminomethylphenol (912573-08-1) + [Y(CH2Si(CH3)2C6H5)3(C4H8O)2] (473595-12-9) → [((Et2NC2H4)2NCH2C6H2-3,5-(CMe3)2-2-O)Y(CH2SiMe2Ph)2]

Guidance literature:

In tetrahydrofuran; byproducts: Si(CH3)3C6H5; (N2); Schlenk technique; soln. of phenol (1 equiv.) in THF was added dropwise to soln. of Y complex in THF; stirred at room temp. for 4 h; volatiles removed (vac.); Et2O added; filtered through Celite; concd. (vac.); recrystd. (petroleum ether); filtered; washed (cold petroleum ether); elem. anal.;

DOI:10.1021/om0608612

upstream raw materials:

formaldehyd

N,N,N',N'-tetraethyldiethylenetriamine

2,4-di-tert-Butylphenol