8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one

Base Information

• Chemical Name: 8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one
• CAS No.: 916892-38-1
• Molecular Formula: C₄₁H₄₃N₇O
• Molecular Weight: 649.839

Synonyms:8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one

Chemical Property of 8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one

There total 1 articles about 8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C19H24N6*CF3CO2H + N-trityl-β-alanine (58995-30-5) → 8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one (916892-38-1)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 25 ℃; for 0.583333h;

DOI:10.1055/s-2006-942502

Reference yield: 55.0%

8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one (916892-38-1) → 8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctane-3-thione

Guidance literature:

With Lawessons reagent; In tetrahydrofuran; at 25 ℃;

DOI:10.1055/s-2006-942502

Reference yield:

8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one (916892-38-1) → N8-benzyl-N8-(1-benzyl-1H-tetrazol-5-yl)-N1-trityl-4-azaoctane-1,8-diamine

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / Lawesson's reagent / tetrahydrofuran / 25 °C

2: 65 percent / NaBH₄; NiCl₂*6H₂O / methanol; tetrahydrofuran / 0.5 h / 25 °C

With Lawessons reagent; sodium tetrahydroborate; nickel dichloride; In tetrahydrofuran; methanol;

DOI:10.1055/s-2006-942502

upstream raw materials:

N-trityl-β-alanine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 916892-38-1 8-[benzyl(1-benzyl-1H-tetrazol-5-yl)amino]-1-(tritylamino)-4-azaoctan-3-one

Send

Send

Metric Ton KG G Pound L ML

Send

Send