Technology Process of C19H22N2O5
There total 1 articles about C19H22N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-(2-amino-5-nitrophenoxy)-butanoic acid ethyl ester; benzaldehyde;
With
sodium tris(acetoxy)borohydride; acetic acid;
In
dichloromethane;
at 20 ℃;
With
sodium hydrogencarbonate;
In
dichloromethane; water;
- Guidance literature:
-
With
iron; ammonium chloride;
In
tetrahydrofuran; water;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: iron; ammonium chloride / tetrahydrofuran; water / Heating / reflux
2: hydrogenchloride; magnesium sulfate / 1,4-dioxane; N,N-dimethyl acetamide / 80 °C
3: hydrogenchloride / 1,4-dioxane; water / 20 h / 20 °C
4: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h
With
hydrogenchloride; iron; magnesium sulfate; ammonium chloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide;