8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-α-L-rhamnopyranosyl-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

Base Information

Chemical Name:8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-α-L-rhamnopyranosyl-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside
CAS No.:114283-96-4
Molecular Formula:C₆₅H₈₁NO₁₇
Molecular Weight:1148.35
Hs Code.:

8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-α-L-rhamnopyranosyl-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

Synonyms:8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-α-L-rhamnopyranosyl-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

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Chemical Property of 8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-α-L-rhamnopyranosyl-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

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Technology Process of 8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-α-L-rhamnopyranosyl-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

There total 27 articles about 8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-α-L-rhamnopyranosyl-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 114283-95-3
8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-(2,4-di-O-acetyl-α-L-rhamnopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

: 114283-96-4
8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-α-L-rhamnopyranosyl-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

Guidance literature:: With sodium methylate; In methanol; for 120h; Ambient temperature;
DOI:10.1016/0008-6215(87)80100-3

Reference yield:

: 34957-73-8
methyl 9-hydroxynonanoate

: 114283-96-4
C₆₅H₈₁NO₁₇

Guidance literature:: Multi-step reaction with 11 steps

1: 59 percent / silver silicate / toluene

4: 77 percent / Hg(CN)2

8: acid

9: 54 percent / Hg(CN)2/HgBr₂ / CH₂Cl₂

10: H₂S

11: NaOMe

With hydrogen sulfide; sodium methylate; mercury(II) cyanide; mercury dibromide; silver silicate; In dichloromethane; toluene;
DOI:10.1016/S0040-4039(00)95120-7

Reference yield:

: 95451-93-7
3,4,6-Tri-O-acetyl-2-azido-2-deoxy-α-D-mannopyranosyl bromide

: 114283-96-4
C₆₅H₈₁NO₁₇

Guidance literature:: Multi-step reaction with 11 steps

1: 59 percent / silver silicate / toluene

4: 77 percent / Hg(CN)2

8: acid

9: 54 percent / Hg(CN)2/HgBr₂ / CH₂Cl₂

10: H₂S

11: NaOMe

With hydrogen sulfide; sodium methylate; mercury(II) cyanide; mercury dibromide; silver silicate; In dichloromethane; toluene;
DOI:10.1016/S0040-4039(00)95120-7