8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-(2,4-di-O-acetyl-α-L-rhamnopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

Base Information

Chemical Name:8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-(2,4-di-O-acetyl-α-L-rhamnopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside
CAS No.:114283-95-3
Molecular Formula:C₆₉H₈₅NO₁₉
Molecular Weight:1232.43
Hs Code.:

8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-(2,4-di-O-acetyl-α-L-rhamnopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

Synonyms:8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-(2,4-di-O-acetyl-α-L-rhamnopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

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Chemical Property of 8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-(2,4-di-O-acetyl-α-L-rhamnopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

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Technology Process of 8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-(2,4-di-O-acetyl-α-L-rhamnopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

There total 25 articles about 8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-(2,4-di-O-acetyl-α-L-rhamnopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34957-73-8
methyl 9-hydroxynonanoate

: 114283-95-3
C₆₉H₈₅NO₁₉

Guidance literature:: Multi-step reaction with 10 steps

1: 59 percent / silver silicate / toluene

4: 77 percent / Hg(CN)2

8: acid

9: 54 percent / Hg(CN)2/HgBr₂ / CH₂Cl₂

10: H₂S

With hydrogen sulfide; mercury(II) cyanide; mercury dibromide; silver silicate; In dichloromethane; toluene;
DOI:10.1016/S0040-4039(00)95120-7

Reference yield:

: 95451-93-7
3,4,6-Tri-O-acetyl-2-azido-2-deoxy-α-D-mannopyranosyl bromide

: 114283-95-3
C₆₉H₈₅NO₁₉

Guidance literature:: Multi-step reaction with 10 steps

1: 59 percent / silver silicate / toluene

4: 77 percent / Hg(CN)2

8: acid

9: 54 percent / Hg(CN)2/HgBr₂ / CH₂Cl₂

10: H₂S

With hydrogen sulfide; mercury(II) cyanide; mercury dibromide; silver silicate; In dichloromethane; toluene;
DOI:10.1016/S0040-4039(00)95120-7

Reference yield:

: 34957-73-8
methyl 9-hydroxynonanoate

: 114283-95-3
8-methoxycarbonyloctyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-3)-O-(2,4-di-O-acetyl-α-L-rhamnopyranosyl)-(1-3)-2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 10 steps

1: 1) silver silicate, molecular sieves / 1) toluene, -20 deg C, 2 h; 2) toluene, -20 deg C, 48 h, then 0 deg C, 75 h

2: 97 percent / NaOMe / methanol / 10 h / Ambient temperature

3: 78 percent / p-toluenesulfonic acid / dimethylformamide / 0.42 h / 60 °C

4: 1) Hg(CN)2 / 1) CH₂Cl₂, 2 h; 2) CH₂Cl₂, room temp., 30 h

5: NaOMe / CH₂Cl₂; methanol / 1 h / Ambient temperature

6: p-TsOH / dimethylformamide / 0.5 h / Ambient temperature

7: pyridine / 5 h / Ambient temperature

8: aq. acetic acid / 0.08 h / Ambient temperature

9: 1) Hg(CN)2, HgBr₂ / 1) CH₂Cl₂, 2 h; 2) CH₂Cl₂, room temp., 21 h

10: H₂S, Et₃N / 1) pyridine, H₂O, room temp., 12 h; 2) pyridine, 0 deg C, 6 h

With molecular sieve; silver silicate; hydrogen sulfide; sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; acetic acid; triethylamine; mercury dibromide; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(87)80100-3