p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate

Base Information

Chemical Name:p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate
CAS No.:122347-84-6
Molecular Formula:C₄₇H₄₄N₃O₁₀PS
Molecular Weight:873.92
Hs Code.:

p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate

Synonyms:p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate

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Chemical Property of p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate

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Technology Process of p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate

There total 4 articles about p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 64370-08-7
p-nitrobenzyl (2R,3R)-2-(benzothiazol-2'-yldithio)-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine-1-acetate

: 13148-05-5
ethyl 3-oxo-4-(triphenylphosphoranylidene)butanoate

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 122347-84-6
p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate

Guidance literature:: In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield:

: 638-07-3
ethyl (2-chloroaceto)acetate

: 122347-84-6
p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.06 percent / benzene / 72 h / Ambient temperature

2: NaHCO₃ / H₂O / 0 - 5 °C

3: 93 percent / tetrahydrofuran / 2 h / Ambient temperature

With sodium hydrogencarbonate; In tetrahydrofuran; water; benzene;

Reference yield:

: 106302-03-8
[3-(ethoxycarbonyl)-2-oxypropyl]triphenylphosphonium chloride

: 122347-84-6
p-nitrobenzyl (2R,3R)-2-<(ethoxycarbonylmethylcarbonyl)(triphenylphosphoranylidene)methylthio>-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine acetate

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / H₂O / 0 - 5 °C

2: 93 percent / tetrahydrofuran / 2 h / Ambient temperature

With sodium hydrogencarbonate; In tetrahydrofuran; water;