C₂₅H₃₀N₆O₃

Base Information

Chemical Name:C₂₅H₃₀N₆O₃
CAS No.:1351753-45-1
Molecular Formula:C₂₅H₃₀N₆O₃
Molecular Weight:462.552
Hs Code.:

C<sub>25</sub>H<sub>30</sub>N<sub>6</sub>O<sub>3</sub>

Synonyms:C₂₅H₃₀N₆O₃

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Chemical Property of C₂₅H₃₀N₆O₃

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Technology Process of C₂₅H₃₀N₆O₃

There total 6 articles about C₂₅H₃₀N₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29682-15-3
methyl 5-bromopicolinate

: 1351753-45-1
C₂₅H₃₀N₆O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride / N,N-dimethyl-formamide / 0.17 h / 140 °C / Inert atmosphere; Microwave irradiation

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate; methanol / 20 - 55 °C

3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide / 0.17 h

4.2: 3 h / 20 °C

5.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

With hydrogenchloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethyl acetate; N,N-dimethyl-formamide; 1.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ml300214g

Reference yield:

: 1401533-33-2
C₃₀H₃₈N₆O₅

: 1351753-45-1
C₂₅H₃₀N₆O₃

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;
DOI:10.1021/ml300214g

Reference yield:

: 375853-82-0,286961-14-6
tert-Butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate

: 1351753-45-1
C₂₅H₃₀N₆O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride / N,N-dimethyl-formamide / 0.17 h / 140 °C / Inert atmosphere; Microwave irradiation

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate; methanol / 20 - 55 °C

3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide / 0.17 h

4.2: 3 h / 20 °C

5.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

With hydrogenchloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethyl acetate; N,N-dimethyl-formamide; 1.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ml300214g