C₂₇H₃₀N₂O₈

Base Information

Chemical Name:C₂₇H₃₀N₂O₈
CAS No.:309743-60-0
Molecular Formula:C₂₇H₃₀N₂O₈
Molecular Weight:510.544
Hs Code.:

C<sub>27</sub>H<sub>30</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₂₇H₃₀N₂O₈

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Chemical Property of C₂₇H₃₀N₂O₈

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Technology Process of C₂₇H₃₀N₂O₈

There total 8 articles about C₂₇H₃₀N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 309743-61-1
dibenzyl 2,7-bis(2-acetoxyethyl)-5-phenyl-3,8-dimethyldipyrrylmethane-1,9-dicarboxylate

: 309743-60-0
C₂₇H₃₀N₂O₈

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 3h; under 2068.59 Torr;

Reference yield:

: 98-88-4
benzoyl chloride

: 309743-60-0
C₂₇H₃₀N₂O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: 45 percent / saturated aqueous NaHCO₃ / CH₂Cl₂ / 20 °C

2.1: SO₂Cl₂ / CCl₄ / 4 h / 45 °C

2.2: 41 percent / AcONa / H₂O; dioxane / 2 h / Heating

3.1: 50 percent / TEA / dimethylformamide / 48 h / 20 °C

4.1: 93 percent / NaBH₄ / methanol; CH₂Cl₂ / 0.5 h / 20 °C

5.1: 79 percent / p-toluenesulfonic acid / CH₂Cl₂ / 1 h / 20 °C

6.1: 87 percent / BF₃*Et₂O; NaBH₄ / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 20 °C

7.1: 96 percent / pyridine / 2 h

8.1: 88 percent / H₂ / 10 percent Pd/C / ethanol / 3 h / 2068.59 Torr

With pyridine; sodium tetrahydroborate; sulfuryl dichloride; TEA; boron trifluoride diethyl etherate; hydrogen; sodium hydrogencarbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; diethylene glycol dimethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 126807-42-9
3-ethoxycarbonylmethyl-2,4-dimethyl-5-benzoylpyrrole

: 309743-60-0
C₂₇H₃₀N₂O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: SO₂Cl₂ / CCl₄ / 4 h / 45 °C

1.2: 41 percent / AcONa / H₂O; dioxane / 2 h / Heating

2.1: 50 percent / TEA / dimethylformamide / 48 h / 20 °C

3.1: 93 percent / NaBH₄ / methanol; CH₂Cl₂ / 0.5 h / 20 °C

4.1: 79 percent / p-toluenesulfonic acid / CH₂Cl₂ / 1 h / 20 °C

5.1: 87 percent / BF₃*Et₂O; NaBH₄ / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 20 °C

6.1: 96 percent / pyridine / 2 h

7.1: 88 percent / H₂ / 10 percent Pd/C / ethanol / 3 h / 2068.59 Torr

With pyridine; sodium tetrahydroborate; sulfuryl dichloride; TEA; boron trifluoride diethyl etherate; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; diethylene glycol dimethyl ether; N,N-dimethyl-formamide;