{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C₂,N}{2-(diphenylphosphino)ethanethiolato-P,S} palladium (II)

Base Information

• Chemical Name: {(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C₂,N}{2-(diphenylphosphino)ethanethiolato-P,S} palladium (II)
• CAS No.: 139276-72-5
• Molecular Formula: 0CH₂Cl₂*C₂₈H₃₀NPPdS
• Molecular Weight: 571.246

Synonyms:{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C₂,N}{2-(diphenylphosphino)ethanethiolato-P,S} palladium (II)

Chemical Property of {(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C₂,N}{2-(diphenylphosphino)ethanethiolato-P,S} palladium (II)

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Technology Process of {(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C₂,N}{2-(diphenylphosphino)ethanethiolato-P,S} palladium (II)

There total 1 articles about {(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C₂,N}{2-(diphenylphosphino)ethanethiolato-P,S} palladium (II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II) (139276-71-4) → {(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{2-(diphenylphosphino)ethanethiolato-P,S} palladium (II) (139276-72-5)

Guidance literature:

With diamino-1,2-ethane; In dichloromethane; water; (N2), stirred (10 min); excess ethylenediamine (water); org. phase sepd.; washed (water); dried (MgSO4); solvent removed; elem. anal.;

Reference yield: 90.0%

{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{2-(diphenylphosphino)ethanethiolato-P,S} palladium (II) (139276-72-5) → {(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{(R/S)-2-((methylthio)-ethyl)diphenylphosphine-P,S} palladium (II) iodide

Guidance literature:

With CH₃I; In dichloromethane; (N2), stirred (1 h); solvent removed; elem. anal.;

upstream raw materials:

chlorobis-{(R)-1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C2,N}{μ-{2-(diphenylphosphino)ethanethiolato-P,S:S}}dipalladium (II)

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