3,3'-(1,2-phenylene)bisacrylic acid

Base Information

Chemical Name:3,3'-(1,2-phenylene)bisacrylic acid
CAS No.:110795-28-3
Molecular Formula:C₁₂H₁₀O₄
Molecular Weight:218.209
Hs Code.:

Synonyms:3,3'-(1,2-phenylene)bisacrylic acid

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Chemical Property of 3,3'-(1,2-phenylene)bisacrylic acid

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Technology Process of 3,3'-(1,2-phenylene)bisacrylic acid

There total 6 articles about 3,3'-(1,2-phenylene)bisacrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 28839-73-8
(E)-3-[2-{(E)-2-ethoxycarbonylvinyl}phenyl]acrylic acid ethyl ester

: 110795-28-3
3,3'-(1,2-phenylene)bisacrylic acid

Guidance literature:: With potassium hydroxide; In ethanol; for 2h; Heating;
DOI:10.1021/jm000107x

Reference yield: 13.0%

: 108-24-7
acetic anhydride

: 643-79-8
o-phthalic dicarboxaldehyde

: 110795-28-3
3,3'-(1,2-phenylene)bisacrylic acid

Guidance literature:: With cesium acetate; at 150 - 160 ℃; for 8h;
DOI:10.1055/s-1987-27880

Reference yield:

: 583-53-9
2,3-dibromobenzene

: 110795-28-3
3,3'-(1,2-phenylene)bisacrylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / Et₃N; 1,3-(diphenylphosphino)propane; Pd(OAc)2 / dimethylformamide / 18 h / 100 °C

2: 91 percent / KOH / ethanol / 2 h / Heating

With palladium diacetate; potassium hydroxide; 1,3-bis-(diphenylphosphino)propane; triethylamine; In ethanol; N,N-dimethyl-formamide; 1: Heck reaction;
DOI:10.1021/jm000107x