α-acetoxymethyl phenyl vinyl ketone

Base Information

Chemical Name:α-acetoxymethyl phenyl vinyl ketone
CAS No.:91962-95-7
Molecular Formula:C₁₂H₁₂O₃
Molecular Weight:204.225
Hs Code.:

Synonyms:α-acetoxymethyl phenyl vinyl ketone

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Chemical Property of α-acetoxymethyl phenyl vinyl ketone

Chemical Property:

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Technology Process of α-acetoxymethyl phenyl vinyl ketone

There total 4 articles about α-acetoxymethyl phenyl vinyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2-((methylthio)methyl)-1-phenylprop-2-en-1-one

: 64-19-7,77671-22-8
acetic acid

: 91962-95-7
α-acetoxymethyl phenyl vinyl ketone

Guidance literature:: With toluene-4-sulfonic acid; In dimethyl sulfoxide; at 150 ℃; for 8h; Inert atmosphere;
DOI:10.1021/acs.orglett.7b02753

Reference yield: 73.0%

: 15121-79-6
2-(hydroxymethyl)-1-phenylprop-2-en-1-one

: 108-24-7
acetic anhydride

: 91962-95-7
α-acetoxymethyl phenyl vinyl ketone

Guidance literature:: In diethyl ether; at 0 ℃;
DOI:10.1016/j.tetlet.2006.07.093

Reference yield:

: 3-(methylthio)-2-((methylthio)methyl)-1-phenylpropan-1-one

: 91962-95-7
α-acetoxymethyl phenyl vinyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: pyrrolidine; toluene-4-sulfonic acid; sodium acetate; acetic acid / dimethyl sulfoxide / 2 h / 150 °C

2: toluene-4-sulfonic acid / dimethyl sulfoxide / 8 h / 150 °C / Inert atmosphere

With pyrrolidine; sodium acetate; toluene-4-sulfonic acid; acetic acid; In dimethyl sulfoxide;
DOI:10.1021/acs.orglett.7b02753