diethylammonium bis(2-phenylethyl)diselenophosphinate

Base Information

• Chemical Name: diethylammonium bis(2-phenylethyl)diselenophosphinate
• CAS No.: 1240500-33-7
• Molecular Formula: C₄H₁₁N*C₁₆H₁₉PSe₂
• Molecular Weight: 473.359
• Mol file: 1240500-33-7.mol

Synonyms:diethylammonium bis(2-phenylethyl)diselenophosphinate

Chemical Property of diethylammonium bis(2-phenylethyl)diselenophosphinate

Chemical Property:

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Technology Process of diethylammonium bis(2-phenylethyl)diselenophosphinate

There total 1 articles about diethylammonium bis(2-phenylethyl)diselenophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

bis(2-phenethyl)phosphine (93017-30-2) + diethylamine (109-89-7) → diethylammonium bis(2-phenylethyl)diselenophosphinate (1240500-33-7)

Guidance literature:

With selenium; In ethanol; at 20 - 60 ℃; Inert atmosphere;

DOI:10.1055/s-0030-1258232

Reference yield: 84.0%

pyridine N-oxide (694-59-7) + diethylammonium bis(2-phenylethyl)diselenophosphinate (1240500-33-7) + zinc dibromide (7699-45-8) → [ZnBr{Se2P(CH2CH2Ph)2}(C5H5NO)]n

Guidance literature:

In acetone; at 20 ℃; for 4h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2015.01.007

upstream raw materials:

bis(2-phenethyl)phosphine

diethylamine