6,7-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranylidenamino)-1H-azepin-3,4,5-tricarbonsaeure-trimethylester

Base Information

Chemical Name:6,7-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranylidenamino)-1H-azepin-3,4,5-tricarbonsaeure-trimethylester
CAS No.:96325-54-1
Molecular Formula:C₃₇H₃₅N₂O₈PS
Molecular Weight:698.733
Hs Code.:

Synonyms:6,7-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranylidenamino)-1H-azepin-3,4,5-tricarbonsaeure-trimethylester

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Chemical Property of 6,7-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranylidenamino)-1H-azepin-3,4,5-tricarbonsaeure-trimethylester

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Technology Process of 6,7-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranylidenamino)-1H-azepin-3,4,5-tricarbonsaeure-trimethylester

There total 3 articles about 6,7-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranylidenamino)-1H-azepin-3,4,5-tricarbonsaeure-trimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 96325-51-8
4,5-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranilidenamino)-3-pyrrolcarbonsaeure-methylester

: 762-42-5
dimethyl acetylenedicarboxylate

: 96325-54-1
6,7-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranylidenamino)-1H-azepin-3,4,5-tricarbonsaeure-trimethylester

Guidance literature:: In acetonitrile; for 2h; Heating;

Reference yield:

: 2526-64-9
dichlorotriphenylphosphorane

: 96325-54-1
6,7-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranylidenamino)-1H-azepin-3,4,5-tricarbonsaeure-trimethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine, hexachloroethane / acetonitrile / 12 h / Ambient temperature

2: 58 percent / acetonitrile / 2 h / Heating

With hexachloroethane; triethylamine; In acetonitrile;

Reference yield:

: 50625-05-3
2-Amino-1-tosyl-Δ²-pyrrolin-3-carbonsaeure-methylester

: 96325-54-1
6,7-Dihydro-1-(4-methylphenylsulfonyl)-2-(triphenylphosphoranylidenamino)-1H-azepin-3,4,5-tricarbonsaeure-trimethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine, hexachloroethane / acetonitrile / 12 h / Ambient temperature

2: 58 percent / acetonitrile / 2 h / Heating

With hexachloroethane; triethylamine; In acetonitrile;