C₂₅H₁₈N₂*ClHO₄

Base Information

Chemical Name:C₂₅H₁₈N₂*ClHO₄
CAS No.:1373752-99-8
Molecular Formula:C₂₅H₁₈N₂*ClHO₄
Molecular Weight:446.89
Hs Code.:

C<sub>25</sub>H<sub>18</sub>N<sub>2</sub>*ClHO<sub>4</sub>

Synonyms:C₂₅H₁₈N₂*ClHO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₁₈N₂*ClHO₄

Chemical Property:

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Technology Process of C₂₅H₁₈N₂*ClHO₄

There total 4 articles about C₂₅H₁₈N₂*ClHO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 765275-26-1
[1,1′:4′,1′′-terphenyl]-2′,3′-diamine

: 100-52-7
benzaldehyde

: 1373752-99-8
C₂₅H₁₈N₂*ClHO₄

Guidance literature:: [1,1′:4′,1′′-terphenyl]-2′,3′-diamine; benzaldehyde; With zirconium(IV) chloride; In chloroform; at 20 ℃; for 24h;

With hydrogenchloride; In tetrahydrofuran; chloroform; water;

With sodium perchlorate; In methanol;
DOI:10.1021/ol300761q

Reference yield:

: 15155-41-6
4,7-dibromobenzo[c][1,2,5]thiadiazole

: 1373752-99-8
C₂₅H₁₈N₂*ClHO₄

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / N,N-dimethyl-formamide; toluene / 24 h / 110 °C / Inert atmosphere

2: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / tetrahydrofuran; ethanol / 20 °C / Reflux

3: zirconium(IV) chloride / chloroform / 24 h / 20 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; cobalt(II) chloride hexahydrate; zirconium(IV) chloride; caesium carbonate; In tetrahydrofuran; ethanol; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol300761q

Reference yield:

: 286380-77-6,287976-96-9
4,7-diphenyl-2,1,3-benzothiadiazole

: 1373752-99-8
C₂₅H₁₈N₂*ClHO₄

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / tetrahydrofuran; ethanol / 20 °C / Reflux

2: zirconium(IV) chloride / chloroform / 24 h / 20 °C

With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; zirconium(IV) chloride; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/ol300761q