(4S,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-one

Base Information

• Chemical Name: (4S,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-one
• CAS No.: 1172135-80-6
• Molecular Formula: C₃₈H₆₀O₄Si
• Molecular Weight: 608.977

Synonyms:(4S,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-one

Chemical Property of (4S,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-one

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Technology Process of (4S,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-one

There total 1 articles about (4S,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(4S,5S,9S,10S,11R,Z)-11-(tert-butyldimethylsilyloxy)-4,10-dimethyl-7-methylene-5,9-bis[(S)-1-phenylethoxy]tridec-2-en-3-yl benzoate (1172135-72-6) → (4S,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-one (1172135-80-6)

Guidance literature:

With methyllithium lithium bromide; In diethyl ether; at -78 ℃; for 2h;

DOI:10.1055/s-0028-1088011

Reference yield: 56.0%

(4S,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-one (1172135-80-6) → (3R,4R,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-ol (1172135-82-8)

Guidance literature:

With L-Selectride; In tetrahydrofuran; at -78 ℃; for 24h;

DOI:10.1055/s-0028-1088011

upstream raw materials:

(4S,5S,9S,10S,11R,Z)-11-(tert-butyldimethylsilyloxy)-4,10-dimethyl-7-methylene-5,9-bis[(S)-1-phenylethoxy]tridec-2-en-3-yl benzoate

Downstream raw materials:

(3R,4R,5S)-7-{(2S,3S,4R)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-methyl-2-[(1S)-1-phenylethoxy]hexyl}-4-methyl-5-[(1S)-1-phenylethoxy]oct-7-en-3-ol

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