N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine

Base Information

Chemical Name:N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine
CAS No.:329069-36-5
Molecular Formula:C₁₆H₁₆N₂O₃
Molecular Weight:284.315
Hs Code.:

Synonyms:N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine

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Technology Process of N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine

There total 1 articles about N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 613-94-5
benzoic acid hydrazide

: 613-45-6
2,4-Dimethoxybenzaldehyde

: 329069-36-5
N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine

Guidance literature:: With acetic acid; In methanol; for 6h; Heating;
DOI:10.1016/j.jorganchem.2003.10.022

Reference yield: 47.0%

: palladium dichloride

: 329069-36-5
N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine

: 676325-88-5
(Pd(C₆H₅CONHNCHC₆H₂(OCH₃)2)Cl)

Guidance literature:: With LiCl; In methanol; mixt. PdCl2 and LiCl in MeOH was refluxed for 1 h, cooled to room temp. and filtered, filtrate was added dropwise to soln. N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine in MeOH and stirred at room temp. for 3 days and refluxed for 3 days; ppt. was filtered, washed with MeOH and dried in air; elem. anal.;
DOI:10.1016/j.jorganchem.2003.10.022