2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylthioacetamide

Base Information

Chemical Name:2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylthioacetamide
CAS No.:1092977-45-1
Molecular Formula:C₂₁H₃₄N₂O₃S
Molecular Weight:394.579
Hs Code.:

Synonyms:2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylthioacetamide

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Chemical Property of 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylthioacetamide

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Technology Process of 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylthioacetamide

There total 7 articles about 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylthioacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 1092977-08-6
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide

: 1092977-45-1
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylthioacetamide

Guidance literature:: With Lawessons reagent; In toluene; for 2h; Reflux;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1092977-45-1
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylthioacetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen bromide / acetic acid / 16 h / 0 - 80 °C

1.2: 16 h / 20 °C

2.1: potassium carbonate / acetone / 72 h / Heating / reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

3.2: 16 h / 20 °C

4.1: Lawessons reagent / toluene / 2 h / Heating / reflux

With Lawessons reagent; hydrogen bromide; sodium hydride; potassium carbonate; In acetic acid; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 132513-29-2
tert-butyl {2-[3-(benzyloxy)phenyl]ethyl}carbamate

: 1092977-45-1
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylthioacetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol / 16 h / 1810.07 Torr

2.1: potassium carbonate / acetone / 72 h / Heating / reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

3.2: 16 h / 20 °C

4.1: Lawessons reagent / toluene / 2 h / Heating / reflux

With Lawessons reagent; hydrogen; sodium hydride; potassium carbonate; palladium 10% on activated carbon; In methanol; N,N-dimethyl-formamide; acetone; toluene;