2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide

Base Information

Chemical Name:2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide
CAS No.:1092977-08-6
Molecular Formula:C₂₁H₃₄N₂O₄
Molecular Weight:378.512
Hs Code.:

Synonyms:2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide

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Chemical Property of 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide

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Technology Process of 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide

There total 6 articles about 2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1092977-07-5
2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamine

: 2675-89-0
2-chloro-N,N-dimethylacetamide

: 1092977-08-6
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide

Guidance literature:: 2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamine; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;

2-chloro-N,N-dimethylacetamide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 16h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1092977-08-6
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen bromide / acetic acid / 16 h / 0 - 80 °C

1.2: 16 h / 20 °C

2.1: potassium carbonate / acetone / 72 h / Heating / reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

3.2: 16 h / 20 °C

With hydrogen bromide; sodium hydride; potassium carbonate; In acetic acid; N,N-dimethyl-formamide; acetone;

Reference yield:

: 29973-97-5
2-(3-benzyloxyphenyl)ethyl amine hydrochloride

: 1092977-08-6
2-(2-(3-butoxyphenyl)-N-tert-butoxycarbonylethylamino)-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 16 h / 1810.07 Torr

3.1: potassium carbonate / acetone / 72 h / Heating / reflux

4.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

4.2: 16 h / 20 °C

With sodium hydroxide; hydrogen; sodium hydride; potassium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone;