(R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide

Base Information

Chemical Name:(R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide
CAS No.:336105-24-9
Molecular Formula:C₁₁H₁₄BrNOS
Molecular Weight:288.208
Hs Code.:

Synonyms:(R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide

Suppliers and Price of (R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide

Chemical Property:

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Technology Process of (R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide

There total 1 articles about (R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1122-91-4
4-bromo-benzaldehyde

: 196929-78-9
(R)-2-methylpropane-2-sulfinamide

: 336105-24-9
(R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide

Guidance literature:: With pyridinium p-toluenesulfonate; magnesium sulfate; In dichloromethane; at 20 ℃;
DOI:10.1016/S0957-4166(02)00099-X

Reference yield: 99.0%

: 106-95-6
allyl bromide

: 336105-24-9
(R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide

: 2-Methyl-propane-2-sulfinic acid [(R)-1-(4-bromo-phenyl)-but-3-enyl]-amide

: 2-Methyl-propane-2-sulfinic acid [(S)-1-(4-bromo-phenyl)-but-3-enyl]-amide

Guidance literature:: With water; zinc; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 20 ℃; for 12h;
DOI:10.1021/ol062216x

Reference yield: 98.0%

: 852447-17-7
tert-butyl 2-(tert-butyldimethylsilyl)-2-oxoacetate

: 100-58-3
phenylmagnesium bromide

: 336105-24-9
(R)-(-)-N-[(1E)-(4-bromophenyl)methylene]-2-methyl-2-propanesulfinamide

: 1508278-74-7
C₂₉H₄₄BrNO₄SSi

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; at -78 ℃; for 1h; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol403388w