6,6'-bis-(2-propoxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-di(phenyl propyl ether)

Base Information

Chemical Name:6,6'-bis-(2-propoxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-di(phenyl propyl ether)
CAS No.:227001-47-0
Molecular Formula:C₃₉H₄₄N₄O₁₂
Molecular Weight:760.798
Hs Code.:

Synonyms:6,6'-bis-(2-propoxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-di(phenyl propyl ether)

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Chemical Property of 6,6'-bis-(2-propoxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-di(phenyl propyl ether)

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Technology Process of 6,6'-bis-(2-propoxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-di(phenyl propyl ether)

There total 4 articles about 6,6'-bis-(2-propoxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-di(phenyl propyl ether) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 59920-13-7
6,6'-bis-(2-hydroxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-diphenol

: 106-94-5
propyl bromide

: 227001-47-0
6,6'-bis-(2-propoxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-di(phenyl propyl ether)

Guidance literature:: With potassium carbonate; In acetone; for 72h; Ambient temperature;

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 227001-47-0
6,6'-bis-(2-propoxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-di(phenyl propyl ether)

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / ZnCl₂ / 4 h / 120 - 130 °C

2: 56 percent / K₂CO₃ / acetone / 72 h / Ambient temperature

With potassium carbonate; zinc(II) chloride; In acetone;

Reference yield:

: 5461-78-9
2-(2-hydroxy-5-nitrobenzyl)-4-nitrophenol

: 227001-47-0
6,6'-bis-(2-propoxy-5-nitrobenzyl)-4,4'-dinitro-2,2'-methanediyl-di(phenyl propyl ether)

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / ZnCO₃, HBr / acetic acid; acetic anhydride / 1) 70 deg C, 20 min, 2) reflux, 4 h

2: 53 percent / ZnCl₂ / 4 h / 120 - 130 °C

3: 56 percent / K₂CO₃ / acetone / 72 h / Ambient temperature

With hydrogen bromide; potassium carbonate; zinc(II) carbonate; zinc(II) chloride; In acetic anhydride; acetic acid; acetone;