6-aminosulfonyl-3-(4-bromophenyl)-5-chloro-1,3,2-benzodithiazolium ylide 1,1-dioxide

Base Information

Chemical Name:6-aminosulfonyl-3-(4-bromophenyl)-5-chloro-1,3,2-benzodithiazolium ylide 1,1-dioxide
CAS No.:1345021-02-4
Molecular Formula:C₁₂H₈BrClN₂O₄S₃
Molecular Weight:455.762
Hs Code.:

Synonyms:6-aminosulfonyl-3-(4-bromophenyl)-5-chloro-1,3,2-benzodithiazolium ylide 1,1-dioxide

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Chemical Property of 6-aminosulfonyl-3-(4-bromophenyl)-5-chloro-1,3,2-benzodithiazolium ylide 1,1-dioxide

Chemical Property:

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Technology Process of 6-aminosulfonyl-3-(4-bromophenyl)-5-chloro-1,3,2-benzodithiazolium ylide 1,1-dioxide

There total 3 articles about 6-aminosulfonyl-3-(4-bromophenyl)-5-chloro-1,3,2-benzodithiazolium ylide 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₁₀BrClN₂O₄S₃

: 1345021-02-4
6-aminosulfonyl-3-(4-bromophenyl)-5-chloro-1,3,2-benzodithiazolium ylide 1,1-dioxide

Guidance literature:: With bromine; In methanol; water; at 20 ℃; for 0.5h;
DOI:10.1016/j.bmc.2011.09.003

Reference yield:

: 121-30-2
chloraminophenamide

: 1345021-02-4
6-aminosulfonyl-3-(4-bromophenyl)-5-chloro-1,3,2-benzodithiazolium ylide 1,1-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; sodium nitrite / acetonitrile / 0 - 40 °C

1.2: 0 - 80 °C

2.1: potassium carbonate / ethanol / 24 h / Reflux

3.1: bromine / methanol; water / 0.5 h / 20 °C

With sulfuric acid; bromine; potassium carbonate; sodium nitrite; In methanol; ethanol; water; acetonitrile;
DOI:10.1016/j.bmc.2011.09.003

Reference yield:

: 74724-36-0
2-bromo-4-chlorobenzene-1,5-disulfonamide

: 1345021-02-4
6-aminosulfonyl-3-(4-bromophenyl)-5-chloro-1,3,2-benzodithiazolium ylide 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / ethanol / 24 h / Reflux

2: bromine / methanol; water / 0.5 h / 20 °C

With bromine; potassium carbonate; In methanol; ethanol; water;
DOI:10.1016/j.bmc.2011.09.003