N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate

Base Information

Chemical Name:N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate
CAS No.:820222-00-2
Molecular Formula:C₂₈H₃₀ClN₇S
Molecular Weight:532.112
Hs Code.:

Synonyms:N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate

Suppliers and Price of N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate

There total 6 articles about N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 5-(4-chlorobenzyl)-2,6-dimethyl-9-(1-naphthyl)-5,9-dihydro[1,3,4]thiadiazolo[2,3-d][1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium iodide

: 109-73-9,85404-21-3
N-butylamine

: 820222-00-2
N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate

Guidance literature:: With triethylamine; In acetonitrile; at -10 - 5 ℃; for 3h;
DOI:10.1016/j.tet.2004.10.081

Reference yield:

: C₂₄H₂₁ClN₆S₂

: 820222-00-2
N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0.5 h / -10 °C

2: tetrahydrofuran / 7 h / 70 - 80 °C

3: CHCl₃ / 24 h / 20 °C

In tetrahydrofuran; chloroform;
DOI:10.1016/j.tet.2004.10.081

Reference yield:

: 7-(4-chloro-benzylamino)-2-methyl-6-(1-methylsulfanyl-ethylideneamino)-5-naphthalen-1-yl-5H-[1,3,4]thiadiazolo[3,2-a][1,3,5]triazin-6-ium; iodide

: 820222-00-2
N-[3-(4-chlorobenzyl)-5-(butylamino)-2-methyl-7-(1-naphthyl)-3,7-dihydro-6H-[1,2,4]triazolo[1,5-a][1,3,5]triazin-8-ium-6-yl]propanimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 7 h / 70 - 80 °C

2: CHCl₃ / 24 h / 20 °C

In tetrahydrofuran; chloroform;
DOI:10.1016/j.tet.2004.10.081