1,1'-(4-Chlorobutylidene)bisbenzene

Base Information

• Chemical Name: 1,1'-(4-Chlorobutylidene)bisbenzene
• CAS No.: 3312-08-1
• Molecular Formula: C16H17 Cl
• Molecular Weight: 244.764
• Hs Code.: 2903999090
• European Community (EC) Number: 221-999-1
• DSSTox Substance ID: DTXSID50186782
• Nikkaji Number: J205.393D
• Wikidata: Q83058175
• Mol file: 3312-08-1.mol

Synonyms:1,1'-(4-Chlorobutylidene)bisbenzene;3312-08-1;(4-chloro-1-phenylbutyl)benzene;EINECS 221-999-1;1,1-diphenyl-4-chlorobutane;1-chloro-4,4-diphenylbutane;4-Chloro-1,1-diphenylbutane;SCHEMBL5635206;DTXSID50186782

Chemical Property of 1,1'-(4-Chlorobutylidene)bisbenzene

Chemical Property:

• Boiling Point: 362.5oC at 760 mmHg
• Flash Point: 164.6oC
• PSA: 0.00000
• Density: 1.061g/cm3
• LogP: 4.83750
• XLogP3: 4.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 5
• Exact Mass: 244.1018782
• Heavy Atom Count: 17
• Complexity: 172

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(CCCCl)C2=CC=CC=C2

Technology Process of 1,1'-(4-Chlorobutylidene)bisbenzene

There total 3 articles about 1,1'-(4-Chlorobutylidene)bisbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4-diphenyl-3-butenyl chloride (5746-95-2) → 1,1-diphenyl-4-chlorobutane (3312-08-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In isopropyl alcohol;

Reference yield:

Diphenylmethane (101-81-5) + 1.3-chlorobromopropane (109-70-6) → 1,1-diphenyl-4-chlorobutane (3312-08-1)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) THF-hexane, 23 deg C, 15 min, 2.) THF, from -78 to 23 deg C, 30 min;

Reference yield:

→ 1,1-diphenyl-4-chlorobutane (3312-08-1)

Guidance literature:

entspr. Cyclopropylcarbinol, HX, H2;

upstream raw materials:

4,4-diphenyl-3-butenyl chloride

Diphenylmethane

1.3-chlorobromopropane

Downstream raw materials:

hydrochloride salt of 1,1-diphenyl-4-n-propylaminobutane

1'-(4,4-diphenylbutyl)-5-chlorospiro[benzofuran-2(3H)4'-piperidine]oxalate

1'-(4,4-diphenylbutyl)spiro[benzofuran-2(3H)4'-piperidine]hydrochloride

1'-(4,4-Diphenylbutyl)-2-methylspiro[2H-1,4-benzodioxepin-3(5H)4'-piperidine]oxalate

Refernces