Technology Process of C24H29BrN2O6S
There total 16 articles about C24H29BrN2O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetra-n-butylammoniumfluoride trihydrate;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sodium hydride / 1,4-dioxane / 0.25 h / 10 °C
1.2: 10 - 100 °C
2.1: sodium hydroxide; water / methanol / 4 h / 50 °C
3.1: potassium carbonate; silver(I) acetate; 1-methyl-pyrrolidin-2-one / 2 h / 110 °C
4.1: bromine; CH3COONa / acetic acid / 1 h / 20 °C
5.1: trifluoroacetic acid / dichloromethane / 20 °C
6.1: 1H-imidazole / tetrahydrofuran / 3 h / 20 °C
7.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C
8.1: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran / 2 h / 20 °C
With
1H-imidazole; 1-methyl-pyrrolidin-2-one; di-isopropyl azodicarboxylate; CH3COONa; water; bromine; silver(I) acetate; sodium hydride; potassium carbonate; tetra-n-butylammoniumfluoride trihydrate; triphenylphosphine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetic acid;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-imidazole / tetrahydrofuran / 3 h / 20 °C
2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C
3: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran / 2 h / 20 °C
With
1H-imidazole; di-isopropyl azodicarboxylate; tetra-n-butylammoniumfluoride trihydrate; triphenylphosphine;
In
tetrahydrofuran;
