methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>hexanoate

Base Information

Chemical Name:methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>hexanoate
CAS No.:122313-69-3
Molecular Formula:C₂₉H₄₁NO₇Si
Molecular Weight:543.733
Hs Code.:

Synonyms:methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>hexanoate

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Chemical Property of methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>hexanoate

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Technology Process of methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>hexanoate

There total 3 articles about methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 122313-68-2
methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-hydroxyhexanoate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 122313-69-3
methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>hexanoate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1021/jo00280a036

Reference yield:

: 84713-20-2
benzyl N-vinylcarbamate

: 122313-69-3
methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>hexanoate

Guidance literature:: Multi-step reaction with 3 steps

2: 92 percent / NaBH₄ / methanol / 7 h / 0 °C

3: 77 percent / imidazole / dimethylformamide / 24 h / Ambient temperature

With 1H-imidazole; sodium tetrahydroborate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00280a036

Reference yield:

: 908810-06-0
methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-oxohexanoate

: 122313-69-3
methyl 3-<<(benzyloxy)carbonyl>amino>-4-carbobenzoxy-5-<<(1,1-dimethylethyl)dimethylsilyl>oxy>hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaBH₄ / methanol / 7 h / 0 °C

2: 77 percent / imidazole / dimethylformamide / 24 h / Ambient temperature

With 1H-imidazole; sodium tetrahydroborate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00280a036