Technology Process of C17H24O3
There total 3 articles about C17H24O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at -78 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/ol402095g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / diethyl ether / 1 h / -20 °C / Inert atmosphere
2.1: tetrahydrofuran; hexane; cyclohexane / 22 h / -78 °C / Inert atmosphere
3.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.5 h / -78 °C / Inert atmosphere
3.2: 4 h / -78 °C / Inert atmosphere
3.3: 2 h / -78 - 20 °C / Inert atmosphere
4.1: boron trifluoride diethyl etherate / dichloromethane / 4 h / -78 °C / Inert atmosphere
With
diethyl methoxy borane; boron trifluoride diethyl etherate; isopropylmagnesium chloride;
In
tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; cyclohexane;
DOI:10.1021/ol402095g
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.5 h / -78 °C / Inert atmosphere
1.2: 4 h / -78 °C / Inert atmosphere
1.3: 2 h / -78 - 20 °C / Inert atmosphere
2.1: boron trifluoride diethyl etherate / dichloromethane / 4 h / -78 °C / Inert atmosphere
With
diethyl methoxy borane; boron trifluoride diethyl etherate;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol402095g
