N,N-dimethylaminogermanate

Base Information

• Chemical Name: N,N-dimethylaminogermanate
• CAS No.: 328061-08-1
• Molecular Formula: C₂H₉GeNO
• Molecular Weight: 135.69
• Mol file: 328061-08-1.mol

Synonyms:N,N-dimethylaminogermanate

Chemical Property of N,N-dimethylaminogermanate

Chemical Property:

Purity/Quality:

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Technology Process of N,N-dimethylaminogermanate

There total 1 articles about N,N-dimethylaminogermanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromogermanate (13569-43-2) + N,N-dimethylhydroxylamine (5725-96-2) → N,N-dimethylaminogermanate (328061-08-1)

Guidance literature:

With n-butyllithium; In Dimethyl ether; pentane; byproducts: LiBr; at -50°C n-butyllithium added dropwise to soln. (CH3)2NOH in pentane; mixt. slowly warmed to ambient temp.; volatiles pumped off; Me2O, H3GeBr condensed onto LiONMe2; mixt. stirred for 10 h at -96°C; isolated by fractionated condensation through cold traps held at -20, -96, -196°C;

DOI:10.1021/ic0007409

upstream raw materials:

bromogermanate

N,N-dimethylhydroxylamine