(2R,3R)-1,1,4,4-tetrakis(4-tert-butylphenyl)-2,3-dimethoxybutane-1,4-diol

Base Information

Chemical Name:(2R,3R)-1,1,4,4-tetrakis(4-tert-butylphenyl)-2,3-dimethoxybutane-1,4-diol
CAS No.:1224853-82-0
Molecular Formula:C₄₆H₆₂O₄
Molecular Weight:678.996
Hs Code.:

Synonyms:(2R,3R)-1,1,4,4-tetrakis(4-tert-butylphenyl)-2,3-dimethoxybutane-1,4-diol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-1,1,4,4-tetrakis(4-tert-butylphenyl)-2,3-dimethoxybutane-1,4-diol

Chemical Property:

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Technology Process of (2R,3R)-1,1,4,4-tetrakis(4-tert-butylphenyl)-2,3-dimethoxybutane-1,4-diol

There total 2 articles about (2R,3R)-1,1,4,4-tetrakis(4-tert-butylphenyl)-2,3-dimethoxybutane-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 27957-93-3
(+)-(2R,3R)-diethyl di-O-methyltartrate

: 3972-65-4
1-bromo-4-tert-butylbenzene

: 1224853-82-0
(2R,3R)-1,1,4,4-tetrakis(4-tert-butylphenyl)-2,3-dimethoxybutane-1,4-diol

Guidance literature:: 1-bromo-4-tert-butylbenzene; With magnesium; In tetrahydrofuran; at 60 ℃; Inert atmosphere;

(+)-(2R,3R)-diethyl di-O-methyltartrate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; ammonium chloride; In tetrahydrofuran; water; Inert atmosphere;
DOI:10.1002/anie.200906550

Reference yield: 67.0%

: 27957-93-3
(+)-(2R,3R)-diethyl di-O-methyltartrate

: 63488-10-8
4-tert-butylmagnesium bromide

: 1224853-82-0
(2R,3R)-1,1,4,4-tetrakis(4-tert-butylphenyl)-2,3-dimethoxybutane-1,4-diol

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja303641p

Reference yield:

: 1224853-82-0
(2R,3R)-1,1,4,4-tetrakis(4-tert-butylphenyl)-2,3-dimethoxybutane-1,4-diol

: C₄₆H₆₀ClO₄P

Guidance literature:: With triethylamine; phosphorus trichloride; In toluene; at 0 - 60 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1002/anie.200906550