(1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane triflate

Base Information

Chemical Name:(1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane triflate
CAS No.:1352143-60-2
Molecular Formula:CHF₃O₃S*C₂₀H₂₆N₂
Molecular Weight:444.518
Hs Code.:

Synonyms:(1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane triflate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane triflate

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Technology Process of (1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane triflate

There total 4 articles about (1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1493-13-6
trifluorormethanesulfonic acid

: 593284-15-2
(1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane

: 1352143-60-2
(1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane triflate

Guidance literature:: In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2011.09.101

Reference yield:

: 915222-02-5
5-[1-((1R,2R)-2-Amino-cyclohexylamino)-ethylidene]-1,3-dimethyl-pyrimidine-2,4,6-trione

: 1352143-60-2
(1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane triflate

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; acetonitrile / 0.75 h

1.2: 0.5 h

2.1: potassium hydroxide / ethanol / 25 h / 50 °C

3.1: dichloromethane / 1 h / 20 °C

With potassium hydroxide; In ethanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2011.09.101

Reference yield:

: 915222-03-6
5-[1-((1R,2R)-2-Dibenzylamino-cyclohexylamino)-ethylidene]-1,3-dimethyl-pyrimidine-2,4,6-trione

: 1352143-60-2
(1R,2R)-N,N-dibenzyl-1,2-diaminocyclohexane triflate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 25 h / 50 °C

2: dichloromethane / 1 h / 20 °C

With potassium hydroxide; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2011.09.101