5-[1-[[(1R,2R)-2-aMinocyclohexyl]aMino]ethylidene]-1,3-diMethyl-2,4,6(1H,3H,5H)-PyriMidinetrione

Base Information

Chemical Name:5-[1-[[(1R,2R)-2-aMinocyclohexyl]aMino]ethylidene]-1,3-diMethyl-2,4,6(1H,3H,5H)-PyriMidinetrione
CAS No.:915222-02-5
Molecular Formula:C14H22N4O3
Molecular Weight:294.354
Hs Code.:
Mol file:915222-02-5.mol

Synonyms:5-[1-[[(1R,2R)-2-aMinocyclohexyl]aMino]ethylidene]-1,3-diMethyl-2,4,6(1H,3H,5H)-PyriMidinetrione

Suppliers and Price of 5-[1-[[(1R,2R)-2-aMinocyclohexyl]aMino]ethylidene]-1,3-diMethyl-2,4,6(1H,3H,5H)-PyriMidinetrione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 5-[1-[[(1R,2R)-2-aMinocyclohexyl]aMino]ethylidene]-1,3-diMethyl-2,4,6(1H,3H,5H)-PyriMidinetrione

Chemical Property:

Melting Point:231 - 233 °C
PSA：95.74000
LogP:1.13730

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 5-[1-[[(1R,2R)-2-aMinocyclohexyl]aMino]ethylidene]-1,3-diMethyl-2,4,6(1H,3H,5H)-PyriMidinetrione

There total 1 articles about 5-[1-[[(1R,2R)-2-aMinocyclohexyl]aMino]ethylidene]-1,3-diMethyl-2,4,6(1H,3H,5H)-PyriMidinetrione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 58713-03-4
5-acetyl-1,3-dimethyl-2,4,6-trioxo-1,3-diazine

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 915222-02-5
5-[1-((1R,2R)-2-Amino-cyclohexylamino)-ethylidene]-1,3-dimethyl-pyrimidine-2,4,6-trione

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.101

Reference yield: 96.0%

: 915222-02-5
5-[1-((1R,2R)-2-Amino-cyclohexylamino)-ethylidene]-1,3-dimethyl-pyrimidine-2,4,6-trione

: 38274-14-5
2,2'-bis-(bromomethyl)-1,1'-biphenyl

: 1352143-58-8
C₂₈H₃₂N₄O₃

Guidance literature:: With potassium carbonate; In acetonitrile; at 60 ℃; for 24h;
DOI:10.1016/j.tet.2011.09.101

Reference yield: 83.0%

: 915222-02-5
5-[1-((1R,2R)-2-Amino-cyclohexylamino)-ethylidene]-1,3-dimethyl-pyrimidine-2,4,6-trione

: 100-52-7
benzaldehyde

: 915222-03-6
5-[1-((1R,2R)-2-Dibenzylamino-cyclohexylamino)-ethylidene]-1,3-dimethyl-pyrimidine-2,4,6-trione

Guidance literature:: 5-[1-((1R,2R)-2-Amino-cyclohexylamino)-ethylidene]-1,3-dimethyl-pyrimidine-2,4,6-trione; benzaldehyde; In water; acetonitrile; for 0.75h;

With sodium cyanoborohydride; In water; acetonitrile; for 0.5h;
DOI:10.1016/j.tet.2011.09.101