(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene

Base Information

Chemical Name:(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene
CAS No.:1428869-48-0
Molecular Formula:C₁₄H₁₂F₆O₅S₂
Molecular Weight:438.369
Hs Code.:

Synonyms:(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene

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Technology Process of (E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene

There total 3 articles about (E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 428-76-2
bis(trifluoromethanesulfonyl)methane

: 1428869-62-8
(E)-3-(3-ethoxyphenyl)acrylaldehyde

: 1428869-48-0
(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene

Guidance literature:: In 1,2-dichloro-ethane; at 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.02.039

Reference yield:

: (E)-3-(3-ethoxyphenyl)-2-propen-1-ol

: 1428869-48-0
(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: manganese(IV) oxide / dichloromethane / 5.5 h / 20 °C / Inert atmosphere

2: 1,2-dichloro-ethane / 3.5 h / 20 °C / Inert atmosphere

With manganese(IV) oxide; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2013.02.039

Reference yield:

: 923955-23-1
m-ethoxy trans-cinnamic acid methyl ester

: 1428869-48-0
(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / hexane; dichloromethane / 4 h / -78 - 0 °C / Inert atmosphere

2: manganese(IV) oxide / dichloromethane / 5.5 h / 20 °C / Inert atmosphere

3: 1,2-dichloro-ethane / 3.5 h / 20 °C / Inert atmosphere

With manganese(IV) oxide; diisobutylaluminium hydride; In hexane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2013.02.039