(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)but-1-en-1-yl)-3-ethoxybenzene

Base Information

Chemical Name:(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)but-1-en-1-yl)-3-ethoxybenzene
CAS No.:1428869-71-9
Molecular Formula:C₁₄H₁₄F₆O₅S₂
Molecular Weight:440.385
Hs Code.:

Synonyms:(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)but-1-en-1-yl)-3-ethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(4,4-bis((trifluoromethyl)sulfonyl)but-1-en-1-yl)-3-ethoxybenzene

Chemical Property:

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Technology Process of (E)-1-(4,4-bis((trifluoromethyl)sulfonyl)but-1-en-1-yl)-3-ethoxybenzene

There total 4 articles about (E)-1-(4,4-bis((trifluoromethyl)sulfonyl)but-1-en-1-yl)-3-ethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1428869-48-0
(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)buta-1,3-dienyl)-3-ethoxybenzene

: 1428869-71-9
(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)but-1-en-1-yl)-3-ethoxybenzene

Guidance literature:: With sodium tetrahydroborate; In ethyl acetate; at -78 ℃; for 1h;

Reference yield:

: (E)-3-(3-ethoxyphenyl)-2-propen-1-ol

: 1428869-71-9
(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)but-1-en-1-yl)-3-ethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: manganese(IV) oxide / dichloromethane / 5.5 h / 20 °C / Inert atmosphere

2.1: 1,2-dichloro-ethane / 3.5 h / 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / ethyl acetate / 1 h / -78 °C / Inert atmosphere

3.2: Inert atmosphere

With manganese(IV) oxide; sodium tetrahydroborate; In dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2013.02.039

Reference yield:

: 1428869-62-8
(E)-3-(3-ethoxyphenyl)acrylaldehyde

: 1428869-71-9
(E)-1-(4,4-bis((trifluoromethyl)sulfonyl)but-1-en-1-yl)-3-ethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,2-dichloro-ethane / 3.5 h / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / ethyl acetate / 1 h / -78 °C / Inert atmosphere

2.2: Inert atmosphere

With sodium tetrahydroborate; In ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2013.02.039